HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 1,3,5-Tris-(p-(dodec-1-yloxycarbonyl)-anilino)-s-triazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Cyanuric chloride | HCID 7954 | — |
| Edukt | Dodecyl 4-aminobenzoate | HCID 328885 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | 1,3,5-Tris-(p-(dodec-1-yloxycarbonyl)-anilino)-s-triazine | HCID 20152739 | — |
Reaktionsbedingungen
| Temperatur | 80 °C |
|---|
Reaktionsschritte
18.5 g of cyanuric chloride and 92 g of dodecyl p-aminobenzoate in 1,000 ml of xylene were heated at 140° C. until HCl gas was no longer evolved. After 8 hours, the reaction solution was cooled to 80° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The precipitated crystals were filtered off under suction and dried.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04617390 |
| Quelldatensatz | uspto-grants-1986_10 |
| ORD ID | ord-b3521faf55594a34a1d0687365b46fe4 |
| Quellennotiz | uspto-grants-1986_10 |