Hydrochloric Acid → HCID 21276884, Verbindung

Reaktionsgleichung

[C:1]1([N:7]2[CH2:16][CH2:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:17]>>[ClH:17].[C:1]1([N:7]2[CH2:16][CH2:15][C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[CH2:8]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Komponenten

Edukt 2

HCID 313Hydrochloric Acid

HCID 11321753HCID 11321753, Verbindung

Produkt 1

HCID 21276884HCID 21276884, Verbindung

Versuchsvorschrift

2-phenyl-1,2,3,4-tetrahydroisoquinoline (0.5 g,) was dissolved in 2M hydrochloric acid (10 ml). The resulting murky solution was cleared by filtering through a pad of diatomaceous earth and freeze-dried when 2-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride was obtained as a yellow glass (670 mg) m.pt. 135°-138° characterised by its nmr spectrum.

Aufarbeitung

filtrationby filtering through a pad of diatomaceous earth
dry with materialfreeze-dried when 2-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Quellen und Nachweise

ORD-Eintrag: ord-deabb8496ccb4e389c3d229b36615370
Quelldatensatz: uspto-grants-1989_01
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04801593

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