HCID 21476957, Verbindung → HCID 21476970, Verbindung
Reaktionsgleichung
[CH2:1]([O:8][C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13]([C:18]([O:20]CC)=[O:19])=[C:12]2[C:23]1[CH:28]=[CH:27][C:26]2[O:29][CH2:30][O:31][C:25]=2[CH:24]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:32]([CH2:37][O:38][C:39]1[CH:46]=[C:45]([O:47][CH3:48])[CH:44]=[CH:43][C:40]=1[CH2:41]Cl)([O:34]CC)=[O:33]>>[CH2:1]([O:8][C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[N:14]([CH2:41][C:40]1[CH:43]=[CH:44][C:45]([O:47][CH3:48])=[CH:46][C:39]=1[O:38][CH2:37][C:32]([OH:34])=[O:33])[C:13]([C:18]([OH:20])=[O:19])=[C:12]2[C:23]1[CH:28]=[CH:27][C:26]2[O:29][CH2:30][O:31][C:25]=2[CH:24]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Komponenten
3
Versuchsvorschrift
5-Benzyloxy-1-(2-carboxymethoxy-4-methoxybenzyl)-3-(3,4-methylenedioxyohenyl)indole-2-carboxylic acid. The title compound was prepared by alkylation of ethyl 5-benzyloxy-3-(3,4-methylenedioxyphenyl)indole-2-carboxylate with 2-carboethoxymethoxy-4-methoxybenzyl chloride followed by saponification using methods previously described in examples 1c and 1d; m.p. 182°-190° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-f73d0a91171641aa9de0da896c465804
- Quelldatensatz
- uspto-grants-1997_11