Hydrochloric Acid → HCID 21473354, Verbindung

HRID 2293994

Reaktionsgleichung

Reaktionsgleichung von HRID 2293994
C(OC([N:8]1[CH2:12][CH:11]([NH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:10]([O:20][CH3:21])[CH2:9]1)=O)(C)(C)C.[ClH:22]>CO>[ClH:22].[CH3:21][O:20][CH:10]1[CH:11]([NH:13][C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH2:12][NH:8][CH2:9]1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 214733421-t-Butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidine

Produkt 1

HCID 21473354HCID 21473354, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

In 100 ml of methanol was dissolved 1.98 g (0.0068 mole) of 1-t-butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidine obtained as described above, and 23.5 ml of 6N hydrochloric acid was added thereto. The mixture was left to stand at room temperature overnight. The solvent was removed under reduced pressure, and the residue was washed with ethanol to obtain 1.71 g of 3-methoxy-4-phenylaminopyrrolidine hydrochloride as white powder.

Aufarbeitung

  1. customobtained
  2. additionwas added
  3. waitThe mixture was left
  4. customThe solvent was removed under reduced pressure
  5. washthe residue was washed with ethanol

Quellen und Nachweise

ORD-Eintrag
ord-0cc71dc497264b3cb7f2d3b3eb386623
Quelldatensatz
uspto-grants-1997_11
Patentnummer
US05688791

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