Aluminium lithium hydride → 3-(8-Phenyloctyloxy)-2-hydroxypropylamine

Beteiligte Stoffe

Reaktionsschritte

A procedure similar to that described in Preparation 13 was repeated, except that 2.6 g of 3-(8-phenyloctyloxy)-2-hydroxypropylazide (Prepared as described in Preparation 65), 0.65 g of lithium aluminum hydride and 80 ml of anhydrous tetrahydrofuran were used, to give 2.11 g of the title compound, melting at 50° C. to 54° C.

Herkunft & Nachweise