HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → Propylene Glycol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | Sodium Methoxide | HCID 10942334 | — |
| Edukt | Propylene glycol methanol | HCID 86614669 | — |
| Lösungsmittel | Propylene Carbonate | HCID 7924 | — |
| Produkt | Propylene Glycol | HCID 1030 | — |
| Produkt | Dimethyl Carbonate | HCID 12021 | — |
Reaktionsschritte
In a process as described in FIG. 1 7 t/h (tonnes per hour) propylene carbonate is fed into the upper part of a reactive distillation zone. Sodium methanolate in 0.5 t/h propylene glycol/methanol mixture as transesterification catalyst is also passed into the upper part of zone in an amount of 0.05 t/h. Twenty t/h methanol, fed into a lower part of the distillation zone, passes upward, and reacts with the propylene carbonate to form propylene glycol product and dimethyl carbonate. The propylene glycol is recovered in an amount of 5 t/h.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07563919B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-92e778977c1649e1ab96e2996ca52116 |
| Quellennotiz | uspto-grants-2009_07 |