HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopropaneacetic acid → N-(Cyclopropylacetyl)-L-alanine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopropaneacetic acid | HCID 138440 | — |
| Edukt | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| Produkt | N-(Cyclopropylacetyl)-L-alanine | HCID 54556694 | — |
Reaktionsschritte
Following General Procedure II-E above using cyclopropylacetic acid (Aldrich) and L-alanine methyl ester hydrochloride (Sigma), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.15 in 25% ethyl acetate/hexanes) and purification was by flash column chromatography using 25% ethyl acetate/hexanes as the eluant.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-c1aa1f135199484289799d0967d68dae |
| Quellennotiz | uspto-grants-2005_02 |