HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,5-Difluorophenylacetic acid → HCID 10391797, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Edukt | 2-(1-Aminoethyl)-1-tert-butoxycarbonyl-4-methoxycarbonyl-4-phenylmethyl-2-imidazoline | HCID 22592461 | — |
| Produkt | HCID 10391797 | HCID 10391797 | — |
Reaktionsschritte
Following General Procedure C above and using 3,5-difluorophenylacetic acid (Aldrich) and 1-tert-butoxycarbonyl-2-(1-aminoethyl)-4-methoxycarbonyl-4-phenylmethyl-2-imidazoline (Example J), the title compound was prepared as an amorphous solid. The reaction was monitored by tlc (Rf=0.34 in 2:1 hexanes/EtOAc) and the product was purified by flash column chromatography.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-5ab1731a61c04d56b1d251826165876c |
| Quellennotiz | uspto-grants-2005_02 |