HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,5-Difluorophenylacetic acid → HCID 178496843, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Edukt | HCID 22592446 | HCID 22592446 | — |
| Produkt | HCID 178496843 | HCID 178496843 | — |
Reaktionsschritte
Following General Procedure C above and using 3,5-difluorophenylacetic acid (Aldrich) and 1-tert-butoxycarbonyl-2-(1-aminoethyl)-4-methoxycarbonyl-4-phenyl-2-imidazoline (Example K), the title compound was prepared as a white foam (90%). The reaction was monitored by tlc (Rf=0.39 in 3:2 hexanes/EtOAc) and the product was purified by flash column chromatography.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-9c6f40ad374f4524be641c8c618468b0 |
| Quellennotiz | uspto-grants-2005_02 |