HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine Methyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dichloroaniline | HCID 7257 | — |
| Edukt | Methyl pyruvate | HCID 11748 | — |
| Produkt | N-(3,4-dichlorophenyl)alanine Methyl Ester | HCID 54289412 | — |
Reaktionsschritte
Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and methyl pyruvate (Aldrich), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.55 in 25% EtOAc/hexanes) and purification was by flash chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-3665ec35c5b94971b7684d4f6339c117 |
| Quellennotiz | uspto-grants-2005_02 |