N-tert-butylhydroxylamine → alpha-(2,4,6-Triethoxyphenyl)-N-tert-butylnitrone
Reaktionsgleichung
[CH2:1]([O:3][C:4]1[CH:11]=[C:10]([O:12][CH2:13][CH3:14])[CH:9]=[C:8]([O:15][CH2:16][CH3:17])[C:5]=1[CH:6]=O)[CH3:2].[C:18]([NH:22][OH:23])([CH3:21])([CH3:20])[CH3:19]>>[CH2:1]([O:3][C:4]1[CH:11]=[C:10]([O:12][CH2:13][CH3:14])[CH:9]=[C:8]([O:15][CH2:16][CH3:17])[C:5]=1[CH:6]=[N+:22]([C:18]([CH3:21])([CH3:20])[CH3:19])[O-:23])[CH3:2]Komponenten
3
Versuchsvorschrift
The title compound was prepared according to the procedure described in Example 11 using 2,4,6-triethoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 92.3% yield as a solid, m.p. 109.1° C.
Aufarbeitung
- customThe title compound was prepared
Quellen und Nachweise
- ORD-Eintrag
- ord-c3a7d6cc1c4747d09792c37f9e7a3e93
- Quelldatensatz
- uspto-grants-2002_08