Sodium Hydroxide → HCID 9925815, Verbindung
Reaktionsgleichung
[Cl:1][C:2]1[C:7]([C:8]#[N:9])=[C:6]([Cl:10])[C:5]([Cl:11])=[C:4]([C:12]#[N:13])[C:3]=1[Cl:14].[OH-:15].[Na+]>C(O)C>[Cl:1][C:2]1[C:3]([Cl:14])=[C:4]([C:12]#[N:13])[C:5]([Cl:11])=[C:6]([Cl:10])[C:7]=1[C:8]([NH2:9])=[O:15]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Tetrachloroterephthalonitrile (26.6 g, 0.1 mol) and ethanol (532 g) were mixed, and the resultant mixture was heated to 79° C. with stirring. To the mixture, a 20% aqueous solution of sodium hydroxide (16 g) was added over six hours. Liquid chromatographic analysis revealed the reaction mixture contained 16.5 g of 2,3,5,6-tetrachloro-4-cyanobenzamide (yield 58%).
Quellen und Nachweise
- ORD-Eintrag
- ord-406130b63c134689a9c2a0bd5cc10f43
- Quelldatensatz
- uspto-grants-2002_08
- Patentnummer
- US06433211B1
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