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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 23049Erstellt: 23. Oktober 2026

Isobutanol → N-(3,5-difluorophenyl)alanine Iso-butyl Ester

https://huagongshe.com/de/reaction/23049

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktIsobutanolHCID 6560—
EduktN-(3,5-difluorophenyl)alanineHCID 53936901—
ProduktN-(3,5-difluorophenyl)alanine Iso-butyl EsterHCID 54289378—

Reaktionsschritte

Following General Procedure AH above and using N-(3,5-difluorophenyl)alanine (from Example AC above) and iso-butanol, the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.9 in 3% methanol/methylene chloride) and purification was by preparative plate chromatography (silica gel using 3% methanol/methylene chloride as the eluant).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06849650B2
Quelldatensatzuspto-grants-2005_02
ORD IDord-d5613df61c1a406e8d4bc734c58fdd6b
Quellennotizuspto-grants-2005_02