HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl pyruvate → N-(3,4-ethylenedioxyphenyl)alanine Iso-butyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl pyruvate | HCID 11748 | — |
| Edukt | N-(3,4-ethylenedioxyphenyl)alanine methyl ester | HCID 53867794 | — |
| Lösungsmittel | Isobutanol | HCID 6560 | — |
| Produkt | N-(3,4-ethylenedioxyphenyl)alanine Iso-butyl Ester | HCID 53856555 | — |
Reaktionsschritte
Following reductive amination General Procedure AA above and using 1,4-benzodioxa-6-amine (Aldrich) and methyl pyruvate (Aldrich), N-(3,4-ethylenedioxyphenyl)alanine methyl ester was prepared. The methyl ester was then transesterified following General Procedure AQ above using iso-butanol to provide the title compound. Purification was by preparative plate chromatography.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-7c12d267fe1f41bd994b7c07dd3a6b03 |
| Quellennotiz | uspto-grants-2005_02 |