2',4'-Dihydroxyacetophenone → 2'-Hydroxy-4'-(ethoxycarbonyldimethylmethoxy)acetophenone

Reaktionsgleichung

[OH:1][C:2]1[CH:7]=[C:6]([OH:8])[CH:5]=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].Br[C:13]([CH3:20])([CH3:19])[C:14]([O:16][CH2:17][CH3:18])=[O:15]>>[OH:1][C:2]1[CH:7]=[C:6]([O:8][C:13]([C:14]([O:16][CH2:17][CH3:18])=[O:15])([CH3:20])[CH3:19])[CH:5]=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10]

Komponenten

Edukt 2

HCID 69902',4'-Dihydroxyacetophenone

HCID 11745Propanoic acid, 2-bromo-2-methyl-, ethyl ester

Produkt 1

HCID 577628812'-Hydroxy-4'-(ethoxycarbonyldimethylmethoxy)acetophenone

Versuchsvorschrift

This compound was synthesized from 2′,4′-dihydroxyacetophenone and ethyl bromoisobutyrate (1 eq) according to general method 4 described earlier.

Quellen und Nachweise

ORD-Eintrag: ord-a5a3265e5a6642e3b21de73ba43b1a62
Quelldatensatz: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07566737B2

Notizen zur Reaktion

Wird geladen…