Ethylene Oxide → HCID 86583625, Verbindung

HRID 2305973

Reaktionsgleichung

Reaktionsgleichung von HRID 2305973
[CH3:1][O:2][CH:3]([CH2:5][O:6][CH:7]([CH2:9][OH:10])[CH3:8])[CH3:4].[OH-].[Na+].[CH2:13]1[O:15][CH2:14]1>>[CH3:1][O:2][CH:3]([CH2:5][O:6][CH:7]([CH2:9][OH:10])[CH3:8])[CH3:4].[CH2:14]1[O:15][CH2:13]1

Komponenten

4

Edukt 3

HCID 6354Ethylene OxideHCID 14798Sodium HydroxideHCID 25485Dipropyleneglycol monomethyl ether

Produkt 1

HCID 86583625HCID 86583625, Verbindung

Reaktionsbedingungen

Temperatur
130 °C

Versuchsvorschrift

An autoclave, as equipped with a thermometer, a stirrer, and a nitrogen-introducing tube, was charged with 74 parts by weight of dipropylene glycol monomethyl ether and 1 part by weight of sodium hydroxide powder, and the internal air of the autoclave was displaced with nitrogen, and then the charged materials were heated to 130° C. Next, 426 parts by weight of ethylene oxide was introduced into the autoclave over a period of 3 hours, and then the resultant reaction mixture was aged at 130° C. for 2 hours and then cooled, thus obtaining a dipropylene glycol monomethyl ether-ethylene oxide adduct (number-average molecular weight=1,000, average molar number of addition=1.94).

Aufarbeitung

  1. customAn autoclave, as equipped with a thermometer, a stirrer
  2. additiona nitrogen-introducing tube
  3. customthe resultant reaction mixture
  4. temperaturecooled

Quellen und Nachweise

ORD-Eintrag
ord-62aef01fc3894abbacaa6bf7479c1c72
Quelldatensatz
uspto-grants-2002_08
Patentnummer
US06441102B2

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