HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Methylethylamine → N-ethyl-N-methyl-2-{4-[3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl]phenyl}acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Methylethylamine | HCID 12219 | — |
| Edukt | {4-[3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl]phenyl}acetic acid | HCID 50992931 | — |
| Produkt | N-ethyl-N-methyl-2-{4-[3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl]phenyl}acetamide | HCID 24827046 | — |
Reaktionsschritte
The title compound was prepared from {4-[3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl]phenyl}acetic acid and N-ethylmethylamine using a similar procedure to that described for Example 13, but purified by flash column chromatography eluting from 0-100% ethyl acetate in hexane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07566735B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-fb37fa22775246bc8c185de260bcd0db |
| Quellennotiz | uspto-grants-2009_07 |