HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Phenylbutyric Acid → N-(4phenylbutanoyl)-L-alanine iso-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Phenylbutyric Acid | HCID 4775 | — |
| Edukt | 2-Methylpropyl (2S)-2-aminopropanoate hydrochloride | HCID 86584981 | — |
| Produkt | N-(4phenylbutanoyl)-L-alanine iso-butyl ester | HCID 15481769 | — |
Reaktionsschritte
Following General Procedure BB and using 4-phenylbutanoic acid (Aldrich) and L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as an oil. The reaction was monitored by tic on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-fb7dd00c26ef4e8ab059239037eb944b |
| Quellennotiz | uspto-grants-2005_02 |