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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2308830Erstellt: 26. Oktober 2026

Ethylene carbonate → 2-(4-(1-Methylethenyl)phenoxy)ethanol

https://huagongshe.com/reaction/2308830

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthylene carbonateHCID 7303—
Eduktp-IsopropenylphenolHCID 584247—
EduktPotassium fluoride dihydrateHCID 23708904—
LösungsmittelDimethylformamideHCID 6228—
Produkt2-(4-(1-Methylethenyl)phenoxy)ethanolHCID 1375061369%

Reaktionsbedingungen

Temperatur150 °C

Reaktionsschritte

A mixture of 20 g p-isopropenylphenol, 1.1 equivalents ethylene carbonate, 0.02 equivalent potassium fluoride dihydrate, and 200 ml N,N-dimethylformamide (DMF) was heated at about 150° C. for about 1.5 hours. After removal of DMF under reduced pressure, the crude product was distilled. 2-(4-(1-Methylethenyl)phenoxy)ethanol, bp 143° C./7 torr, was obtained as a white solid in 69% yield.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04691042
Quelldatensatzuspto-grants-1987_09
ORD IDord-ab2fa38553ff41ddaac4e08279e66ef0
Quellennotizuspto-grants-1987_09