HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2308830Erstellt: 26. Oktober 2026
Ethylene carbonate → 2-(4-(1-Methylethenyl)phenoxy)ethanol
https://huagongshe.com/reaction/2308830
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Ethylene carbonate | HCID 7303 | — |
| Edukt | p-Isopropenylphenol | HCID 584247 | — |
| Edukt | Potassium fluoride dihydrate | HCID 23708904 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 2-(4-(1-Methylethenyl)phenoxy)ethanol | HCID 13750613 | 69% |
Reaktionsschritte
A mixture of 20 g p-isopropenylphenol, 1.1 equivalents ethylene carbonate, 0.02 equivalent potassium fluoride dihydrate, and 200 ml N,N-dimethylformamide (DMF) was heated at about 150° C. for about 1.5 hours. After removal of DMF under reduced pressure, the crude product was distilled. 2-(4-(1-Methylethenyl)phenoxy)ethanol, bp 143° C./7 torr, was obtained as a white solid in 69% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04691042 |
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| Quelldatensatz | uspto-grants-1987_09 |
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| ORD ID | ord-ab2fa38553ff41ddaac4e08279e66ef0 |
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| Quellennotiz | uspto-grants-1987_09 |
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