(3-Bromophenyl)acetic acid → 2-[(3-bromophenyl)acetamido]butyric Acid isobutyl Ester

HRID 23091

Reaktionsgleichung

Reaktionsgleichung von HRID 23091
[Br:1][C:2]1[CH:3]=[C:4]([CH2:8][C:9]([OH:11])=O)[CH:5]=[CH:6][CH:7]=1.[NH2:12][CH:13]([CH2:21][CH3:22])[C:14]([O:16][CH2:17][CH:18]([CH3:20])[CH3:19])=[O:15]>>[CH2:17]([O:16][C:14](=[O:15])[CH:13]([NH:12][C:9](=[O:11])[CH2:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([Br:1])[CH:3]=1)[CH2:21][CH3:22])[CH:18]([CH3:19])[CH3:20]

Komponenten

3

Edukt 2

HCID 74653(3-Bromophenyl)acetic acidHCID 13743360Isobutyl 2-aminobutyrate

Produkt 1

HCID 154817712-[(3-bromophenyl)acetamido]butyric Acid isobutyl Ester

Versuchsvorschrift

Following General Procedure BI above and using 3-bromophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure BJ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.

Aufarbeitung

  1. customThe reaction was monitored by tlc on silica gel and purification
  2. filtrationwas by filtration

Quellen und Nachweise

ORD-Eintrag
ord-de94374137c442c2a1b821818cbfa633
Quelldatensatz
uspto-grants-2005_02
Patentnummer
US06849650B2

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