HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methyl-1-butanol → N-(phenylacetyl)valine 2-methylbutyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methyl-1-butanol | HCID 8723 | — |
| Edukt | (2S)-3-methyl-2-(2-phenylacetamido)butanoic acid | HCID 853958 | — |
| Produkt | N-(phenylacetyl)valine 2-methylbutyl Ester | HCID 15481773 | — |
Reaktionsschritte
Following General Procedure BC and using the N-(phenylacetyl) valine prepared in Step A above and 2-methylbutan-1-ol (Aldrich), the title compound was prepared as a diastereomeric mixture. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849650B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-234b2d2cfd5742799503095206a222bd |
| Quellennotiz | uspto-grants-2005_02 |