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HRID 231005Erstellt: 25. Oktober 2026

4,4'-Dihydroxybiphenyl → 4'-(2-Methylbutoxy)(1,1'-biphenyl)-4-ol

https://huagongshe.com/reaction/231005

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4,4'-DihydroxybiphenylHCID 7112—
EduktPotassium CarbonateHCID 11430—
Edukt1-Bromo-2-methylbutaneHCID 25254—
LösungsmittelEthanolHCID 702—
Produkt4'-(2-Methylbutoxy)(1,1'-biphenyl)-4-olHCID 1409381558%

Reaktionsschritte

A solution of 0.20 mole(37.2 g) of 4,4'-dihydroxybiphenyl, 0.10 mole(15.1 g) of the above 2-methyl-1-bromobutane, and 0.60 mole(33.7 g) of potassium carbonate in 300 ml of ethanol was refluxed for 16 hours. After the reaction, the reaction solution was filtered and concentrated, then purified by column chromatography to obtain 4.9 g of 4'-(2-methylbutoxy)-4-hydroxybiphenyl. (yield: 58%)

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04844835
Quelldatensatzuspto-grants-1989_07
ORD IDord-7579d4eec5224c2fa2bdb88004109b17
Quellennotizuspto-grants-1989_07