Ethanol → Ethyl 4'-hydroxy-4-biphenylcarboxylate

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Ethanol	HCID 702	—
Edukt	Sulfuric Acid	HCID 1118	—
Edukt	4'-Hydroxy-4-biphenylcarboxylic acid	HCID 301556	—
Produkt	Ethyl 4'-hydroxy-4-biphenylcarboxylate	HCID 4049156	97%

Reaktionsschritte

1 ml of conc. sulfuric acid was added to an ethanol solution of 0.1 mole(21.4 g) of 4'-hydroxybiphenyl-4-carboxylic acid, and stirred for 18 hours. The reaction solution was concentrated, and then purified by column chromatography, to obtain 22.8 g of 4'-hydroxybiphenyl-4-carboxylic acid ethyl ester [m.p. 144.4°-145.6° C⟧ (yield: 97%)

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04844835
Quelldatensatz	uspto-grants-1989_07
ORD ID	ord-ba5b307958374a14ab8e0e363ac9ecfd
Quellennotiz	uspto-grants-1989_07