HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → 9,10-Dihydroanthracene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | Anthracene | HCID 8418 | — |
| Edukt | Cerium | HCID 23974 | — |
| Lösungsmittel | 1,2-Dimethoxyethane | HCID 8071 | — |
| Produkt | 9,10-Dihydroanthracene | HCID 11940 | 59% |
Reaktionsschritte
1.14 mmole of anthracene is reacted with 4.57 m atoms of cerium as powder in 7.5 ml of DME in the conditions of example 9 with application of ultrasound, thus producing anthracenecerium. After action of a methanol excess and the usual treatment, 9,10-dihydroanthracene was isolated with a yield of 59%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04845201 |
| Quelldatensatz | uspto-grants-1989_07 |
| ORD ID | ord-4d94dcbf8d314500877ef0fa80aacbef |
| Quellennotiz | uspto-grants-1989_07 |