2,2-Dinitropropanol → 2,2-Dinitropropyl pentafluorothioacetate

Reaktionsgleichung

[N+:1]([C:4]([N+:8]([O-:10])=[O:9])([CH3:7])[CH2:5][OH:6])([O-:3])=[O:2].[F:11][S:12]([F:19])=[C:13](O)[C:14]([F:17])([F:16])[F:15]>>[F:11][S:12]([F:19])=[C:13]([O:6][CH2:5][C:4]([N+:8]([O-:10])=[O:9])([N+:1]([O-:3])=[O:2])[CH3:7])[C:14]([F:17])([F:16])[F:15]

Komponenten

Edukt 2

HCID 701942,2-Dinitropropanol

HCID 86743239Pentafluorothioacetic acid

Produkt 1

HCID 570728572,2-Dinitropropyl pentafluorothioacetateAusbeute 95 %

Versuchsvorschrift

Using a method similar to example 12, 2,2-dinitropropanol and pentafluorothioacetic acid were reacted to form 2,2-dinitropropyl pentafluorothioacetate (95% yield) mp 22° C.;

Aufarbeitung

customwere reacted

Quellen und Nachweise

ORD-Eintrag: ord-be8d5bcb41ba4e8da3e8c2e3987231fc
Quelldatensatz: uspto-grants-1989_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04849540

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