Sodium Hydroxide → inositol 1,2,6-triphosphate

HRID 232391

Reaktionsgleichung

Reaktionsgleichung von HRID 232391
[CH:1]1([O:32][P:33]([O-:36])([O-:35])=[O:34])[CH:6]([O:7][P:8]([O-:11])([O-:10])=[O:9])[CH:5]([O:12][P:13]([O-:16])([O-:15])=[O:14])[CH:4]([O:17]P([O-])([O-])=O)[CH:3]([O:22]P([O-])([O-])=O)[CH:2]1[O:27]P([O-])([O-])=O.[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[OH-].[Na+]>C(O)C>[C@H:4]1([OH:17])[CH:3]([OH:22])[C@@H:2]([OH:27])[C@@H:1]([O:32][P:33]([OH:36])([OH:35])=[O:34])[CH:6]([O:7][P:8]([OH:10])([OH:11])=[O:9])[C@@H:5]1[O:12][P:13]([OH:15])([OH:16])=[O:14]

Komponenten

4

Edukt 2

HCID 14798Sodium HydroxideHCID 66391Phytate Persodium

Produkt 1

HCID 65762inositol 1,2,6-triphosphate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

100 ml of the fraction containing D-myo-inositol-1.2.6-triphosphate obtained in Example 15 was neutralized to a pH of about 7 with an aqueous solution of NaOH. After addition of 100 ml ethanol the volume of the solution was reduced by evaporation and the sodiumsalt was precipitated, centrifuged, recrystallized and dried in vacuum. The purified sodiumsalt of D-myo-inositol-1.2.6-triphosphate obtained was structurally confirmed by analysis with H-NMR.

Aufarbeitung

  1. customwas reduced by evaporation
  2. customthe sodiumsalt was precipitated
  3. customrecrystallized
  4. customdried in vacuum

Quellen und Nachweise

ORD-Eintrag
ord-bc91b0ea600744548cec0081e6df62c8
Quelldatensatz
uspto-grants-1989_07
Patentnummer
US04851560

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