Hydrochloric Acid → 4-(5-Aminopentyl)phenol-hydrochloride

HRID 232817Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 232817
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13]C)=[CH:9][CH:8]=1.[ClH:15]>>[ClH:15].[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]1[CH:8]=[CH:9][C:10]([OH:13])=[CH:11][CH:12]=1

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 11507342HCID 11507342, Verbindung

Produkt 1

HCID 194336454-(5-Aminopentyl)phenol-hydrochloride

Versuchsvorschrift

20.8 g of 4-(5-aminopentyl)anisole are heated with 350 ml of semiconcentrated hydrochloric acid in a glass bomb for 10 hours to 180° C. The solution is concentrated by evaporation in vacuo, the residue is dissolved in ethanol and treated with activated charcoal. The residue remaining after evaporation is used further as a crude product.

Aufarbeitung

  1. concentrationThe solution is concentrated by evaporation in vacuo
  2. dissolutionthe residue is dissolved in ethanol
  3. additiontreated with activated charcoal
  4. customafter evaporation

Quellen und Nachweise

ORD-Eintrag
ord-78fd134132fb4aaab3a5e00ac3de4fca
Quelldatensatz
uspto-grants-1997_01
Patentnummer
US05591769

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