HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 232877Erstellt: 24. Oktober 2026
Ethanethiol → 2-(7-Chloro-6-ethylthioquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine
https://huagongshe.com/de/reaction/232877
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Ethanethiol | HCID 6343 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 2-(7-Chloro-6-fluoroquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine | HCID 23359142 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 2-(7-Chloro-6-ethylthioquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine | HCID 23359231 | — |
Reaktionsschritte
0.37 ml of ethyl mercaptan and 1.12 g of potassium carbonate were added to 2.0 g of 2-(7-chloro-6-fluoroquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine dissolved in 80 ml of dimethylformamide and the mixture was stirred at 90° C. for 4 hours.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05591752 |
|---|
| Quelldatensatz | uspto-grants-1997_01 |
|---|
| ORD ID | ord-173c904036b3494ca7a6e3278b1b792f |
|---|
| Quellennotiz | uspto-grants-1997_01 |
|---|
