Dimethylformamide → HCID 11122592, Verbindung
Reaktionsgleichung
[CH3:1][N:2]1[C@H:11]2[CH2:12][C:13]3[C:14](=[CH:15][C:16]([O:20][CH3:21])=[C:17]([OH:19])[CH:18]=3)[C:9]3[C:10]2=[C:5]([CH:6]=[C:7]([OH:24])[C:8]=3[O:22][CH3:23])[CH2:4][CH2:3]1.C(Cl)[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1.[CH3:33]N(C=O)C>>[CH3:33][N:2]([CH2:1][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[CH2:11][CH2:12][C:13]1[C:14]2[CH:9]=[CH:10][C:5]3[C:4]([C:15]=2[C:16]([O:20][CH3:21])=[C:17]([OH:19])[CH:18]=1)=[CH:3][C:8]([O:22][CH3:23])=[C:7]([OH:24])[CH:6]=3Komponenten
4
Versuchsvorschrift
1 g of boldine was dissolved in 30 ml of (DMF), the mixture was reacted with 1.2 ml of benzyl chloride at 100°-110° C. for 2 hrs. The residue obtained after evaporation under reduced pressure was purified to give the pure compound (5) N-benzylsecoboldine.
Aufarbeitung
- customThe residue obtained
- customafter evaporation under reduced pressure
- customwas purified