Monochloramine → 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride

HRID 2351022Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2351022
[CH3:1][CH:2]1[O:7][CH:6]([CH3:8])[CH2:5][N:4]([CH2:9][CH:10](O)C)[CH2:3]1.[Cl:13]N>>[ClH:13].[Cl:13][CH2:10][CH2:9][N:4]1[CH2:3][CH:2]([CH3:1])[O:7][CH:6]([CH3:8])[CH2:5]1

Komponenten

3

Edukt 2

HCID 25423MonochloramineHCID 98999alpha,2,6-Trimethylmorpholin-4-ylethanol

Produkt 1

HCID 129555394-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride

Versuchsvorschrift

An amount, 389.3 grams, of 2,6-dimethyl-N-(2-hydroxypropyl) morpholine (2.25 moles) was condensed with the free chloroamine obtained from 481.5 grams N-chloroethyl-2,6-dimethylmorpholine hydrochloride (2.25 moles) as described above to give 415.9 grams (58.8%) of the catalyst, bp 127°-129° C. at 0.3 mm of Hg. The structure was confirmed as that of the title compound by elemental analysis, calc. 64.9 C, 10.9 H, 8.9 N; found 64.4 C, 10.6 H, 8.9 N.

Quellen und Nachweise

ORD-Eintrag
ord-3b7003df5f774f039e097d636cbed4ef
Quelldatensatz
uspto-grants-1989_10
Patentnummer
US04871845

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