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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2351251Erstellt: 27. Oktober 2026

Aniline → Aniline, N-(2,2,2-trifluoroethyl)-

https://huagongshe.com/reaction/2351251

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAnilineHCID 6115—
EduktHCID 10993805HCID 10993805—
LösungsmittelDichloromethaneHCID 6344—
ProduktAniline, N-(2,2,2-trifluoroethyl)-HCID 959690,8%

Reaktionsschritte

250 mg (0.573 mmol) of (2,2,2-trifluoroethyl)phenyliodonium trifluoromethanesulfonate, 107 mg (1.15 mmol) of aniline and 5 ml of methylene chloride were reacted and worked up in the same manner as described in Reference Example 4 to obtain 91.1 mg of N-(2,2,2-trifluoroethyl)aniline as an oily substance. Yield, 92%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04873027
Quelldatensatzuspto-grants-1989_10
ORD IDord-5d456a4c84e6411aa1338919de3e5b1a
Quellennotizuspto-grants-1989_10