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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2352037Erstellt: 26. Oktober 2026

Methanol → Methyl 2,3-dihydro-1H-pyrrolizine-1-carboxylate

https://huagongshe.com/reaction/2352037

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethanolHCID 887—
Edukt2,3-Dihydro-1h-pyrrolizine-1-carboxylic acidHCID 12795105—
LösungsmittelHydrochloric AcidHCID 313—
ProduktMethyl 2,3-dihydro-1H-pyrrolizine-1-carboxylateHCID 12795075—

Reaktionsschritte

2,3-Dihydro-1H-pyrrolo[1,2-a]pyrrole-1-carboxylic acid is dissolved in methanol containing a small amount of concentrated hydrochloric acid. The resulting solution is heated to reflux, and then cooled. The title compound is isolated by rotary evaporation of the solvent under reduced pressure, and may be purified by chromatography on silica gel with hexane/ethyl acetate as eluent.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04874871
Quelldatensatzuspto-grants-1989_10
ORD IDord-586d422b14554575a5537722250183b1
Quellennotizuspto-grants-1989_10