HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Edukt | CID 11268547 | HCID 11268547 | — |
| Edukt | 12-{[(Prop-2-en-1-yloxy)carbonyl]amino}dodecanoic acid | HCID 11652337 | — |
| Lösungsmittel | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Produkt | 2-Dimethylaminopyridine | HCID 21885 | — |
Reaktionsschritte
Following a procedure similar to that described in Example 12, but using 547 mg of radicicol, 3.75 g of 12-allyloxycarbonylaminododecanoic acid, 15 ml of dry 1-methyl-2-pyrrolidinone, 1.6 g of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 418 mg of the title compound were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05597846 |
| Quelldatensatz | uspto-grants-1997_01 |
| ORD ID | ord-0d49396f87aa4d0694bd0c6068091e57 |
| Quellennotiz | uspto-grants-1997_01 |