Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
Reaktionsgleichung
[CH3:1][C@H]1OC(=O)C2C(O)=CC(O)=C(Cl)C=2CC(=O)C=CC=C[C@H]2O[C@H]2C1.C1(CCCCCC(O)=O)C=CC=CC=1.[CH:40]1([N:46]=[C:47]=[N:48][CH:49]2[CH2:54][CH2:53][CH2:52]CC2)CCCCC1>O1CCCC1>[CH3:1][N:46]([C:47]1[CH:52]=[CH:53][CH:54]=[CH:49][N:48]=1)[CH3:40]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Following a procedure similar to that described in Example 12, but using 500 mg of radicicol, 659 mg of 6-phenylhexanoic acid, 15 ml of dry tetrahydrofuran, 707 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 704 mg of the title compound were obtained.
Quellen und Nachweise
- ORD-Eintrag
- ord-a55bdd3068da47d19b5a11ac1a9e7294
- Quelldatensatz
- uspto-grants-1997_01
- Patentnummer
- US05597846
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