HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dodecanenitrile → 4-Ethyl-2-undecyl-2-oxazoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dodecanenitrile | HCID 17092 | — |
| Edukt | 2-Amino-1-butanol | HCID 22129 | — |
| Katalysator | Cadmium acetate, dihydrate | HCID 6537495 | — |
| Lösungsmittel | 1-Butanol | HCID 263 | — |
| Produkt | 4-Ethyl-2-undecyl-2-oxazoline | HCID 226848 | 89,6% |
Reaktionsschritte
25 g (137.9 mmoles) of undecyl cyanide was treated with 15.2 ml (165 mmoles) of DL-2-amino-1-butanol in presence of 919 mg (3.54 mmoles) of cadmium acetate dihydrate in 1-butanol as outlined under Example 1. 31.31g (89.6%) of product was obtained on distillation at 124°-125°C./1.2-1.4mmHg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04876249 |
| Quelldatensatz | uspto-grants-1989_10 |
| ORD ID | ord-1faa8d722da24280a9e2d67bb1575a23 |
| Quellennotiz | uspto-grants-1989_10 |