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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 235276Erstellt: 23. Oktober 2026

Water → HCID 178419936, Verbindung

https://huagongshe.com/de/reaction/235276

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktWaterHCID 962—
Edukt2-NaphthalenecarbonitrileHCID 11944—
EduktSodium AzideHCID 33557—
EduktLithium ChlorideHCID 433294—
Lösungsmittel2-MethoxyethanolHCID 8019—
ProduktHCID 178419936HCID 178419936—

Reaktionsschritte

A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05597925
Quelldatensatzuspto-grants-1997_01
ORD IDord-137d0e3b02b449b0bb19965f452b207a
Quellennotizuspto-grants-1997_01