HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → HCID 178419936, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | 2-Naphthalenecarbonitrile | HCID 11944 | — |
| Edukt | Sodium Azide | HCID 33557 | — |
| Edukt | Lithium Chloride | HCID 433294 | — |
| Lösungsmittel | 2-Methoxyethanol | HCID 8019 | — |
| Produkt | HCID 178419936 | HCID 178419936 | — |
Reaktionsschritte
A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05597925 |
| Quelldatensatz | uspto-grants-1997_01 |
| ORD ID | ord-137d0e3b02b449b0bb19965f452b207a |
| Quellennotiz | uspto-grants-1997_01 |