Water → HCID 178419936, Verbindung

HRID 235276

Reaktionsgleichung

Reaktionsgleichung von HRID 235276
[C:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1)#[N:2].[N-:13]=[N+:14]=[N-:15].[Na+].[Cl-].[Li+].O>COCCO>[CH:4]1[C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[CH:11]=[CH:12][C:3]=1[C:1]1[NH:15][N:14]=[N:13][N:2]=1

Komponenten

6

Edukt 4

HCID 962WaterHCID 119442-NaphthalenecarbonitrileHCID 33557Sodium AzideHCID 433294Lithium Chloride

Produkt 1

HCID 178419936HCID 178419936, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 80192-MethoxyethanolLösungsmittel

Versuchsvorschrift

A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.

Aufarbeitung

  1. customwas placed in a reaction vessel
  2. temperatureThe above mixture was refluxed

Quellen und Nachweise

ORD-Eintrag
ord-137d0e3b02b449b0bb19965f452b207a
Quelldatensatz
uspto-grants-1997_01
Patentnummer
US05597925

Verknüpfte Notizen

Wird geladen…