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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 235319Erstellt: 25. Oktober 2026

Methanol → 4-(3-tert-Butyl-4-methoxybenzoyloxyethyl)benzenemethanol

https://huagongshe.com/reaction/235319

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethanolHCID 887—
EduktTetrahydrofuranHCID 8028—
EduktSodium borohydrideHCID 4311764—
Edukt4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehydeHCID 21474525—
LösungsmittelWaterHCID 962—
Produkt4-(3-tert-Butyl-4-methoxybenzoyloxyethyl)benzenemethanolHCID 53848055—

Reaktionsschritte

1.6 g (5 mmol) of the aldehyde obtained in Example 45, 50 ml of THF and 50 ml of methanol are introduced into a round-bottomed flask. 100 mg (2.5 mmol) of sodium borohydride are added in small portions and the mixture is stirred at room temperature for 4 h. The reaction medium is poured into water, the mixture is extracted with ethyl ether and the organic phase is separated after settling has taken place, dried over magnesium sulphate and evaporated.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05597839
Quelldatensatzuspto-grants-1997_01
ORD IDord-9f4bd2205b2e42ceba968bdc02156d6e
Quellennotizuspto-grants-1997_01