HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tryptamine hydrochloride → (S)-N-Benzyl-N-methyl-2-[[2-(1H-indol-3-yl)-ethylamino]-N'-(t-butoxycarbonyl)-ethylamino]-3-phenyl-propionamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tryptamine hydrochloride | HCID 67652 | — |
| Edukt | (S)-N-benzyl-N-methyl-2-[N-(t-butoxycarbonyl)-2-oxo-ethylamino]-3-phenyl-propionamide | HCID 53842533 | — |
| Produkt | (S)-N-Benzyl-N-methyl-2-[[2-(1H-indol-3-yl)-ethylamino]-N'-(t-butoxycarbonyl)-ethylamino]-3-phenyl-propionamide | HCID 86750252 | — |
Reaktionsschritte
Prepare by the method of Example 1 using 2-(1H-indol-3-yl)-ethylamine hydrochloride salt (tryptamine hydrochloride salt) (0.197 g, 1.0 mmol) and (S)-N-benzyl-N-methyl-2-[N-(t-butoxycarbonyl)-2-oxo-ethylamino]-3-phenyl-propionamide (0.41 g, 1.0 mmol) to give the title compound: TLC Rf =0.69 (silica gel, 85% chloroform/10% methanol/5% acetic acid).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05597845 |
| Quelldatensatz | uspto-grants-1997_01 |
| ORD ID | ord-0003ab746bf54a9f8ba8d633e3decd4c |
| Quellennotiz | uspto-grants-1997_01 |