HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
9,10-Dihydro-9,10-dioxo-1-anthracenesulfonic acid → Silver 9,10-anthraquinone-1-sulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 9,10-Dihydro-9,10-dioxo-1-anthracenesulfonic acid | HCID 6713 | — |
| Edukt | Silver(II) oxide | HCID 92152 | — |
| Edukt | Sodium anthraquinone-1-sulfonate | HCID 517266 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Silver 9,10-anthraquinone-1-sulfonate | HCID 86625862 | — |
Reaktionsschritte
Five parts of sodium 9,10-anthraquinone-1-sulfonate was dissolved in 400.0 parts of ion-exchanged water at 45° C. The obtained solution was, passed through a column packed with 6.9 parts of an ion-exchanged resin (DUOLITE C20) to obtain a solution containing 9,10-anthraquinone-1-sulfonic acid. To the obtained solution, 2.0 parts' of silver oxide was added and the resultant mixture was stirred over night. The mixture was filtrated to obtain 3.9 parts of silver 9,10-anthraquinone-1-sulfonate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07759045B2 |
| Quelldatensatz | uspto-grants-2010_07 |
| ORD ID | ord-d6eb375e76004d959da9c09b1d49e6d2 |
| Quellennotiz | uspto-grants-2010_07 |