HCID 59389336, Verbindung → HCID 59389321, Verbindung
Reaktionsgleichung
[OH:1][CH2:2][C:3]1[C:4]2[N:5]([N:12]=[C:13]([C:15]([F:18])([F:17])[F:16])[CH:14]=2)[C:6]([CH2:9][O:10][CH3:11])=[CH:7][CH:8]=1>C(Cl)(Cl)Cl.[O-2].[O-2].[Mn+4]>[CH3:11][O:10][CH2:9][C:6]1[N:5]2[N:12]=[C:13]([C:15]([F:18])([F:17])[F:16])[CH:14]=[C:4]2[C:3]([CH:2]=[O:1])=[CH:8][CH:7]=1Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Reaktionsbedingungen
- Temperatur
- 50 °C
Versuchsvorschrift
Activated manganese dioxide (20.0 g) was added to a solution of the compound of Example 326 (6.00 g) in chloroform (120 mL). The reaction mixture was stirred at 50° C. for 5 hours. Subsequently, the mixture was filtered through Celite. The filtrate was concentrated to afford the title compound as a pale yellow powder (5.74 g).