4-Chloro-alpha,alpha,alpha-trifluoro-3-nitrotoluene → 2-Nitro-1-phenoxy-4-(trifluoromethyl)benzene

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A mixture of 3.8 g of methyl phenyl carbonate, 5.64 g of 4-chloro-3-nitrobenzotrifluoride, and 0.17 g of TBPB was heated at 150° C. for 1 hour. All of the carbonate was converted with a 99 percent yield of 2-nitro-4-trifluoromethylphenyl phenyl ether. Distillation of the product yielded 6.65 g (94 percent) of the ether, b.p. 148°-9° C./2 mm.

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