HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 8-Hydroxy-2-methyl-7-quinolinecarboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | 8-Hydroxy-2-methyl-7-quinolinecarboxylic acid methyl ester | HCID 54511211 | — |
| Produkt | 8-Hydroxy-2-methyl-7-quinolinecarboxamide | HCID 21271472 | — |
Reaktionsschritte
8-Hydroxy-2-methyl-7-quinolinecarboxylic acid methyl ester is reacted with excess ammonia in a steel bomb for 12-18 hr. The excess ammonia is allowed to evaporate and the residue is crystallized from a suitable solvent to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04642343 |
| Quelldatensatz | uspto-grants-1987_02 |
| ORD ID | ord-833cdc1c912c44cfbecbe45644db9f04 |
| Quellennotiz | uspto-grants-1987_02 |