HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trimethylsilanol → Hexamethyldisiloxane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trimethylsilanol | HCID 66110 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | Hexamethyldisiloxane | HCID 24764 | — |
Reaktionsschritte
This reaction proceeds slowly without diethylether but reacts faster at reflux temperatures. Trimethylsilanol is condensed during the HMDS distillation step to give HMDSO, which reacts as shown above.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04644076 |
| Quelldatensatz | uspto-grants-1987_02 |
| ORD ID | ord-5481fd3911d649d58cd82ef099a34174 |
| Quellennotiz | uspto-grants-1987_02 |