HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester → HCID 178419570, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester | HCID 20216369 | — |
| Edukt | HCID 178513045 | HCID 178513045 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178419570 | HCID 178419570 | 94,9% |
Reaktionsschritte
A mixture of 17.17 gm of ethyl N-[3-(2-bromoacetyl)-phenyl]-carbamate, 7.1 gm of amidinothiourea and 45 ml of ethanol was refluxed for 4 hours and then cooled to room temperature. The precipitate formed thereby was filtered off and washed with cold ethanol, yielding 22 gm of the title compound, m.p. 240°-2° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04645841 |
| Quelldatensatz | uspto-grants-1987_02 |
| ORD ID | ord-6d885af43e5a42df8c8026180f6c9d4f |
| Quellennotiz | uspto-grants-1987_02 |