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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 236641Erstellt: 25. Oktober 2026

Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester → HCID 178419570, Verbindung

https://huagongshe.com/reaction/236641

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktCarbamic acid, [3-(bromoacetyl)phenyl]-, ethyl esterHCID 20216369—
EduktHCID 178513045HCID 178513045—
LösungsmittelEthanolHCID 702—
ProduktHCID 178419570HCID 17841957094,9%

Reaktionsschritte

A mixture of 17.17 gm of ethyl N-[3-(2-bromoacetyl)-phenyl]-carbamate, 7.1 gm of amidinothiourea and 45 ml of ethanol was refluxed for 4 hours and then cooled to room temperature. The precipitate formed thereby was filtered off and washed with cold ethanol, yielding 22 gm of the title compound, m.p. 240°-2° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04645841
Quelldatensatzuspto-grants-1987_02
ORD IDord-6d885af43e5a42df8c8026180f6c9d4f
Quellennotizuspto-grants-1987_02