Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2367078Erstellt: 25. Oktober 2026

2-Bromoethanol → 1-(2-Hydroxyl-ethyl)-3-vinyl imidazolium bromide

https://huagongshe.com/reaction/2367078

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-BromoethanolHCID 10898—
Edukt1-VinylimidazoleHCID 66171—
EduktImidazolium cationHCID 444234—
LösungsmittelTolueneHCID 1140—
Produkt1-(2-Hydroxyl-ethyl)-3-vinyl imidazolium bromideHCID 86699448—

Reaktionsschritte

With reference to FIG. 4, 0.14 mmloe of 1-vinylimidazole, being the imidazolium liquid monomer, and 50 ml of toluene are mixed to obtain a mixture, followed by sequentially dropping 0.16 mmole of 2-bromoethanol into the mixture to trigger off an alkylation of the 1-vinylimidazole and the 2-bromoethanol. Then, a solution with two phase of layering is obtained after three days of reaction, wherein the lower layer of the solution is further isolated and repeatedly washed by toluene and ether, followed by being condensed and dried in vacuo for 1 hour, to obtain 1-(2-hydroxyl-ethyl)-3-vinylimidazolium bromide (also known as HEVIMB).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08697884B2
Quelldatensatzuspto-grants-2014_04
ORD IDord-8865d8a7ddc443ec8842b5f538ac4f3b
Quellennotizuspto-grants-2014_04