17-Aminoheptadecanoic acid tert-butyl ester → 15-Aminopentadecanoic acid tert-butyl ester

HRID 2369798Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2369798
[C:1]([O:5][C:6](=[O:24])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]CCN)([CH3:4])([CH3:3])[CH3:2].C(OC(COC(C[NH:37]CC(O)=O)=O)=O)(C)(C)C>>[C:1]([O:5][C:6](=[O:24])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][NH2:37])([CH3:4])([CH3:3])[CH3:2]

Komponenten

3

Edukt 2

HCID 8664712917-Aminoheptadecanoic acid tert-butyl esterHCID 86647132(Tert-butoxycarbonylmethoxycarbonylmethylamino) acetic acid

Produkt 1

HCID 8664713115-Aminopentadecanoic acid tert-butyl ester

Versuchsvorschrift

15-Aminopentadecanoic acid tert-butyl ester was prepared in analogous fashion to 17-aminoheptadecanoic acid tert-butyl ester, and was coupled to (tert-butoxycarbonylmethoxycarbonylmethylamino) acetic acid in analogous fashion to the method described in Example 1, step 4.

Quellen und Nachweise

ORD-Eintrag
ord-9f3ebed907a349c4a214f7ee9e6a4231
Quelldatensatz
uspto-grants-2014_04
Patentnummer
US08710000B2

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