HCID 46947540, Verbindung → HCID 46947721, Verbindung

HRID 2370589Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2370589
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])C(F)(F)F)=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:41])([F:40])[F:39])[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCCCC(F)(F)[F:64])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O>>[CH3:43][C:2]1([CH3:1])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:64])[F:26])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:40])([F:41])[F:39])[CH:30]=2)[C:3]1=[O:42]

Komponenten

3

Edukt 2

HCID 46947540HCID 46947540, VerbindungHCID 46947720HCID 46947720, Verbindung

Produkt 1

HCID 46947721HCID 46947721, VerbindungAusbeute 73 %

Versuchsvorschrift

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 12 replacing the compound of Example 1. A pale yellow oil is obtained with a yield of 73% (140 mg).

Aufarbeitung

  1. customA pale yellow oil is obtained with a yield of 73% (140 mg)

Quellen und Nachweise

ORD-Eintrag
ord-350ac0f647b44297a99ff8f16af2025d
Quelldatensatz
uspto-grants-2014_04
Patentnummer
US08710091B2

Notizen zur Reaktion

Wird geladen…