HCID 46944971, Verbindung → HCID 46944972, Verbindung

HRID 2370590Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2370590
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19]CC(F)(F)C(F)(F)F)=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:41])([F:40])[F:39])[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCC[C:62]([F:74])([F:73])[C:63]([F:72])([F:71])[C:64]([F:70])([F:69])[C:65]([F:68])([F:67])[F:66])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O>>[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][C:62]([F:74])([F:73])[C:63]([F:71])([F:72])[C:64]([F:69])([F:70])[C:65]([F:68])([F:67])[F:66])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:39])([F:41])[F:40])[CH:30]=2)[C:3]1=[O:42]

Komponenten

3

Edukt 2

HCID 46944971HCID 46944971, VerbindungHCID 46947540HCID 46947540, Verbindung

Produkt 1

HCID 46944972HCID 46944972, VerbindungAusbeute 85 %

Versuchsvorschrift

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 14 replacing the compound of Example 1. A pale yellow oil is obtained with a yield of 85% (145 mg).

Aufarbeitung

  1. customA pale yellow oil is obtained with a yield of 85% (145 mg)

Quellen und Nachweise

ORD-Eintrag
ord-91463e120e5b486687652ee19ef089a5
Quelldatensatz
uspto-grants-2014_04
Patentnummer
US08710091B2

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