HCID 46944973, Verbindung → HCID 46945366, Verbindung

HRID 2370595Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2370595
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:12](=[O:13])[C:11]([CH3:15])([CH3:14])[N:10]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][S:25][CH2:26][CH2:27][CH2:28][C:29]([F:35])([F:34])[C:30]([F:33])([F:32])[F:31])[C:9]2=[O:36])=[CH:4][C:3]=1[C:37](F)(F)F.CC1(C)N(CCCCCCCCCSCCCC(F)(F)C(F)(F)F)C(=O)N(C2C=CC([N+]([O-])=O)=C(C)C=2)C1=O>>[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:12](=[O:13])[C:11]([CH3:15])([CH3:14])[N:10]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][S:25][CH2:26][CH2:27][CH2:28][C:29]([F:35])([F:34])[C:30]([F:33])([F:31])[F:32])[C:9]2=[O:36])=[CH:4][C:3]=1[CH3:37]

Komponenten

3

Edukt 2

HCID 46944973HCID 46944973, VerbindungHCID 46945364HCID 46945364, Verbindung

Produkt 1

HCID 46945366HCID 46945366, VerbindungAusbeute 93 %

Versuchsvorschrift

The experimental protocol is the same as that described for the compound of Example 16, the compound of Example 23 replacing the compound of Example 1. The expected compound is obtained in the form of a brown oil with a yield of 93%.

Quellen und Nachweise

ORD-Eintrag
ord-f75695261e524897aa549cd7b2004c31
Quelldatensatz
uspto-grants-2014_04
Patentnummer
US08710091B2

Notizen zur Reaktion

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